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香豆素_91-64-5
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香豆素

BW903033 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨詢'}} ¥{{goodObj.sell_price || 0}} 咨詢 91-64-5 100mg {{goodObj.date}} 秦境 {{item.norm}} 98.2% {{inventory}}
香豆素介紹:

Reference Material

This certificate is designed in accordance with ISO17034 and ISO Guide 31. This reference material (RM) was designed,produced andverified in accordance with ISO/IEC 17025, ISO 17034 and a registered qualitymanagement system ISO9001.

Method of Characterisation

GC/FID

Batch Information

Water Content: <0.1% (by Karl-Fischer-Titration)

Uncertainty

The certified value(s) and uncertainty(ies) aredetermined in accordance with ISO 17034 with an 95% confidence level (k=2).Uncertainty is based on the Total Combined Uncertainty, including uncertaintiesof characterisation, homogeneity and stability testing. Stability values are basedon real evidence opposed to simulation.

The producer certifies that this reference materialmeets the specification stated in this certificate until the expiry date,provided it is stored unopened at the recommended temperature herein. Productwarranties for this reference material are set out in the terms and conditionsof purchase.

Intended Use

This RM is intended for use in a laboratory as acalibration and quality control standard or in method development foranalytical techniques.

Safety

Proper precautions should be observed whilehandling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements arecalibrated with weights traceable to the national standards (DKD). Thecalibration of the balances is verified daily internally and annually by anexternal7 accredited calibration service. Chromatographic methods are traceableto the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RMhave been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealedcontainer at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum samplesize and if less material is used, to increase the certified uncertainty by afactor of two for half sample and four for a quarter of sample. If storageafter opening is necessary, the RM should be tightly closed and kept from lightand moisture. If the RM was in a sealed ampoule, it should be transferred to avial with minimum head space.


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國(guó)家標(biāo)準(zhǔn): 食品安全國(guó)家標(biāo)準(zhǔn) 食品中香豆素的測(cè)定
標(biāo)準(zhǔn)名稱及標(biāo)準(zhǔn)號(hào) GB 5009.34-2022 食品安全國(guó)家標(biāo)準(zhǔn) 食品中香豆素的測(cè)定
適用范圍 適用于食品(如飲料、糕點(diǎn)、調(diào)味品等)中香豆素含量的測(cè)定,檢測(cè)限范圍為0.01 mg/kg~10 mg/kg。
核心檢測(cè)方法 高效液相色譜-熒光檢測(cè)法(HPLC-FLD),以乙腈-水為流動(dòng)相,C18色譜柱分離,激發(fā)波長(zhǎng)280 nm,發(fā)射波長(zhǎng)450 nm。
檢出限與定量限 方法檢出限(LOD)為0.005 mg/kg,定量限(LOQ)為0.015 mg/kg。
質(zhì)控樣品要求 每批次樣品需加標(biāo)平行樣,回收率應(yīng)控制在80%~120%;空白試驗(yàn)中不得檢出目標(biāo)物。
關(guān)鍵實(shí)驗(yàn)步驟 1. 樣品經(jīng)乙腈超聲提取;
2. 提取液過(guò)0.22 μm濾膜;
3. 進(jìn)樣量10 μL,柱溫30℃;
4. 外標(biāo)法定量。
特別說(shuō)明 避免使用含香豆素的本底污染容器;熒光檢測(cè)器需定期校準(zhǔn);樣品需避光保存。
行業(yè)標(biāo)準(zhǔn): 進(jìn)出口化妝品中香豆素的測(cè)定
標(biāo)準(zhǔn)名稱及標(biāo)準(zhǔn)號(hào) SN/T 5357-2021 進(jìn)出口化妝品中香豆素的測(cè)定
適用范圍 適用于膏霜、乳液、香水等化妝品中香豆素的檢測(cè),定量限為0.5 mg/kg。
核心檢測(cè)方法 氣相色譜-質(zhì)譜聯(lián)用法(GC-MS),DB-5MS色譜柱,程序升溫,選擇離子監(jiān)測(cè)模式(SIM)。
質(zhì)控樣品要求 每批次樣品需包含1個(gè)空白對(duì)照及2個(gè)加標(biāo)平行樣,相對(duì)標(biāo)準(zhǔn)偏差(RSD)應(yīng)≤10%。

以上信息僅供參考,請(qǐng)以相應(yīng)標(biāo)準(zhǔn)的原文為準(zhǔn)!

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