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氯氰菊酯_52315-07-8,氯氰菊酯
圖片僅供參考,具體產(chǎn)品以實物為準!

氯氰菊酯

BW902010 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨詢'}} ¥{{goodObj.sell_price || 0}} 咨詢 52315-07-8 100mg {{goodObj.date}} 秦境 {{item.norm}} 95.8% {{inventory}}
氯氰菊酯介紹:

Reference Material

This certificate is designed in accordance with ISO17034 and ISO Guide 31. This reference material (RM) was designed,produced andverified in accordance with ISO/IEC 17025, ISO 17034 and a registered qualitymanagement system ISO9001.

Product Name

Cypermethrin

Product Code

BW902010

Lot Number

23051511

CAS No.

52315-07-8

Mol. Formula

C22H19Cl2NO3

Mol. Weight

416.30

Certified on

26 May 2023

Expiry Date

25May 2025

Storage Temp

20°C ± 4°C

Specification

100 mg

CERTIFIED

Purity

CERTIFIED

Expanded Uncertainty (U)

Approved by

95.8%

0.8%

Method of Characterisation

GC/FID

Uncertainty

The certified value(s) and uncertainty(ies) aredetermined in accordance with ISO 17034 with an 95% confidence level (k=2).Uncertainty is based on the Total Combined Uncertainty, including uncertaintiesof characterisation, homogeneity and stability testing. Stability values arebased on real evidence opposed to simulation.

The producer certifies that this reference materialmeets the specification stated in this certificate until the expiry date,provided it is stored unopened at the recommended temperature herein. Productwarranties for this reference material are set out in the terms and conditionsof purchase.

Intended Use

This RM is intended for use in a laboratory as acalibration and quality control standard or in method development foranalytical techniques.

Safety

Proper precautions should be observed whilehandling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements arecalibrated with weights traceable to the national standards (DKD). Thecalibration of the balances is verified daily internally and annually by anexternal accredited calibration service. Chromatographic methods are traceableto the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RMhave been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealedcontainer at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum samplesize and if less material is used, to increase the certified uncertainty by a factorof two for half sample and four for a quarter of sample. If storage afteropening is necessary, the RM should be tightly closed and kept from light andmoisture. If the RM was in a sealed ampoule, it should be transferred to a vialwith minimum head space.


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手機版:氯氰菊酯

本公司銷售的所有產(chǎn)品僅供實驗科研使用,不用于人體及臨床診斷。

國家標準解讀:《食品安全國家標準 植物源性食品中氯氰菊酯殘留量的測定》
標準名稱及標準號GB 23200.113-2018《食品安全國家標準 植物源性食品中氯氰菊酯殘留量的測定》
適用范圍適用于蔬菜、水果、谷物等植物源性食品中氯氰菊酯及其異構體殘留量的檢測。
核心檢測方法氣相色譜-質(zhì)譜聯(lián)用法(GC-MS),采用內(nèi)標法定量,通過提取、凈化、濃縮等步驟測定目標物。
檢出限與定量限檢出限(LOD)為0.01 mg/kg,定量限(LOQ)為0.03 mg/kg,滿足農(nóng)殘限量管控要求。
質(zhì)控樣品要求每批次樣品需加標回收實驗,空白樣品中添加濃度應為LOQ的1~5倍,回收率需控制在70%~120%。
關鍵實驗步驟1. 樣品均質(zhì)化后用乙腈提取;2. 通過固相萃取柱(SPE)凈化;3. 氮吹濃縮至干后用丙酮復溶;4. 上機分析,保留時間和特征離子定性定量。
特別說明檢測過程中需注意氯氰菊酯的同分異構體分離問題,建議使用毛細管色譜柱(如DB-5MS)優(yōu)化分離條件。

以上信息僅供參考,請以相應標準的原文為準!

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