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滅多威(EC 17025)_16752-77-5,滅多威
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滅多威(EC 17025)

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滅多威介紹:

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

Method of Characterisation

GC/FID

Batch Information

Water Content: <0.1% (by Karl-Fischer-Titration)

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.

Tel:029-85836892 Web:www.qjbzwz.com Email:[email protected]

Address:Jiawei Technology Industry Base, Aerospace East Road, Xi’an , Shaanxi Province


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國(guó)家標(biāo)準(zhǔn)解讀:滅多威(CAS:16752-77-5)相關(guān)檢測(cè)標(biāo)準(zhǔn)
標(biāo)準(zhǔn)名稱(chēng)及標(biāo)準(zhǔn)號(hào) GB 23200.113-2018 食品安全國(guó)家標(biāo)準(zhǔn) 植物源性食品中208種農(nóng)藥及其代謝物殘留量的測(cè)定 液相色譜-質(zhì)譜聯(lián)用法
適用范圍 適用于植物源性食品中滅多威及其他農(nóng)藥殘留的定量檢測(cè),包括蔬菜、水果、谷物等基質(zhì)。
核心檢測(cè)方法 采用液相色譜-串聯(lián)質(zhì)譜法(LC-MS/MS),通過(guò)保留時(shí)間和特征離子對(duì)定性,外標(biāo)法定量。
檢出限與定量限 滅多威的檢出限(LOD)為0.005 mg/kg,定量限(LOQ)為0.01 mg/kg。
質(zhì)控樣品要求 每批次樣品需包含空白基質(zhì)加標(biāo)樣品(添加濃度0.01-0.1 mg/kg),回收率應(yīng)控制在70%-120%,相對(duì)標(biāo)準(zhǔn)偏差(RSD)≤20%。
關(guān)鍵實(shí)驗(yàn)步驟 1. 樣品前處理:乙腈提取,QuEChERS法凈化;
2. 儀器條件:C18色譜柱,流動(dòng)相為0.1%甲酸水溶液和乙腈;
3. 質(zhì)譜參數(shù):多反應(yīng)監(jiān)測(cè)模式(MRM),母離子m/z 163.1,子離子m/z 88.1和106.1。
特別說(shuō)明 滅多威易水解,樣品提取后需在24小時(shí)內(nèi)完成檢測(cè);基質(zhì)效應(yīng)需通過(guò)空白基質(zhì)匹配校準(zhǔn)曲線進(jìn)行補(bǔ)償。
其他相關(guān)行業(yè)標(biāo)準(zhǔn)參考
標(biāo)準(zhǔn)名稱(chēng)及標(biāo)準(zhǔn)號(hào) GB 2763-2021 食品安全國(guó)家標(biāo)準(zhǔn) 食品中農(nóng)藥最大殘留限量
關(guān)聯(lián)內(nèi)容 規(guī)定滅多威在各類(lèi)食品中的最大殘留限量(如谷物中限量為0.02 mg/kg),檢測(cè)結(jié)果需符合該標(biāo)準(zhǔn)要求。

以上信息僅供參考,請(qǐng)以相應(yīng)標(biāo)準(zhǔn)的原文為準(zhǔn)!

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