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環(huán)己烷_110-82-7
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環(huán)己烷

BW901034 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨詢'}} ¥{{goodObj.sell_price || 0}} 咨詢 110-82-7 1mL {{goodObj.date}} 秦境 {{item.norm}} 99.9% {{inventory}}
環(huán)己烷介紹:

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external7 accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.

Tel:029-85836892 Web:www.qjbzwz.com Email:[email protected]

Address:Jiawei Technology Industry Base, Aerospace East Road, Xi’an , Shaanxi Province


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本公司銷售的所有產(chǎn)品僅供實(shí)驗(yàn)科研使用,不用于人體及臨床診斷。

1. 標(biāo)準(zhǔn)名稱及標(biāo)準(zhǔn)號(hào)
標(biāo)準(zhǔn)名稱:環(huán)境空氣 揮發(fā)性有機(jī)物的測(cè)定 罐采樣/氣相色譜-質(zhì)譜法
標(biāo)準(zhǔn)號(hào):HJ 644-2013
2. 適用范圍
本標(biāo)準(zhǔn)規(guī)定了環(huán)境空氣中揮發(fā)性有機(jī)物(包括環(huán)己烷)的罐采樣結(jié)合氣相色譜-質(zhì)譜聯(lián)用(GC-MS)的檢測(cè)方法,適用于環(huán)境空氣和污染源無組織排放中揮發(fā)性有機(jī)物的測(cè)定。
3. 核心檢測(cè)方法
使用惰性材質(zhì)采樣罐采集樣品,經(jīng)預(yù)濃縮儀富集后,通過氣相色譜分離,質(zhì)譜檢測(cè)器進(jìn)行定性和定量分析。環(huán)己烷在DB-5MS色譜柱中保留時(shí)間為5.3分鐘,特征離子為84、55、56。
4. 檢出限與定量限
環(huán)己烷的檢出限為0.2 μg/m3(以采樣體積100 L計(jì)),定量限為0.5 μg/m3。需根據(jù)實(shí)際采樣體積調(diào)整計(jì)算結(jié)果。
5. 質(zhì)控樣品要求
每批次樣品需至少包含1個(gè)實(shí)驗(yàn)室空白樣和1個(gè)平行樣。標(biāo)準(zhǔn)曲線相關(guān)系數(shù)需≥0.995,加標(biāo)回收率應(yīng)控制在80%-120%,否則需重新分析。
6. 關(guān)鍵實(shí)驗(yàn)步驟
(1) 使用經(jīng)高溫老化處理的采樣罐,避免污染;
(2) 樣品在預(yù)濃縮儀中去除水蒸氣后富集;
(3) GC升溫程序:初始40℃保持2分鐘,以5℃/min升至120℃,再以10℃/min升至250℃;
(4) 質(zhì)譜采用全掃描模式(Scan)或選擇離子模式(SIM)采集數(shù)據(jù)。
7. 特別說明
環(huán)己烷易揮發(fā)且易燃,需在低溫(<4℃)避光保存樣品。分析前需確認(rèn)色譜柱極性是否適用,避免與共流出物干擾。實(shí)驗(yàn)操作應(yīng)符合實(shí)驗(yàn)室安全規(guī)范(如GB/T 27476)。

以上信息僅供參考,請(qǐng)以相應(yīng)標(biāo)準(zhǔn)的原文為準(zhǔn)!

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