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樂果_60-51-5,樂果
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樂果

BW902022 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨詢'}} ¥{{goodObj.sell_price || 0}} 咨詢 60-51-5 10mg {{goodObj.date}} 秦境 {{item.norm}} 98.5% {{inventory}}
樂果介紹:

REFERENCE MATERIAL CERTIFICATE

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

Product Name

Dimethoate

Product Code

BW902022

Lot Number

25041513

CAS No.

60-51-5

Mol. Formula

C5H12NO3PS2

Mol. Weight

229.26

Certified on

9 Apr. 2025

Expiry Date

8 Apr. 2030

Storage Temp

-18°C ± 5°C

Specification

10mg

CERTIFIED

Purity

CERTIFIED

Expanded Uncertainty (U)

Approved by

98.5%

1.0%

Method of Characterisation

GC/FID

Batch Information

Water Content: <0.1% (by Karl-Fischer-Titration)

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.


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標準匹配結(jié)果
GB 23200.113-2018 食品安全國家標準 植物源性食品中208種農(nóng)藥及其代謝物殘留量的測定
標準名稱及標準號
GB 23200.113-2018 氣相色譜-質(zhì)譜聯(lián)用法檢測樂果等208種農(nóng)藥殘留的核心標準
適用范圍
適用于水果、蔬菜及谷物中樂果的定量分析,基質(zhì)覆蓋葉菜類、根莖類和漿果類
核心檢測方法
氣相色譜-質(zhì)譜法(GC-MS) 配備電子轟擊電離源(EI),采用選擇離子監(jiān)測(SIM)模式,樂果特征離子為87/125/229
檢出限與定量限
方法檢出限(LOD) 0.005 mg/kg(以樣品基質(zhì)計)
定量限(LOQ) 0.01 mg/kg
質(zhì)控樣品要求
空白加標回收率 70%-120%(添加濃度需≥LOQ)
平行樣偏差 ≤20%(低濃度) / ≤15%(高濃度)
關(guān)鍵實驗步驟
樣品前處理 乙腈震蕩提取→QuEChERS凈化→氮吹濃縮定容
色譜條件 DB-5MS色譜柱(30m×0.25mm×0.25μm),進樣口溫度250℃,程序升溫梯度
特別說明
1. 標準要求檢測器響應(yīng)值需≥3倍信噪比
2. 需定期進行基質(zhì)效應(yīng)驗證試驗
3. 建議每12小時重新校準儀器
```

以上信息僅供參考,請以相應(yīng)標準的原文為準!

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