四氫呋喃
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REFERENCE MATERIAL CERTIFICATE
Reference Material
This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.
Product Name
Custom-Tetrahydrofuran
Product Code
BW901110
Lot Number
23091516
CAS No.
109-99-9
Mol. Formula
C4H8O
Mol. Weight
72.11
Certified on
13 Sep 2023
Expiry Date
12 Sep 2026
Storage Temp
20°C ± 4°C
Specification
1g
CERTIFIED
Purity
CERTIFIED
Expanded Uncertainty (U)
Approved by
99.6%
1.0%
Uncertainty
The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.
The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.
Intended Use
This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.
Safety
Proper precautions should be observed while handling. See Safety Data Sheet.
Traceability
The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).
Homogeneity
Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.
Storage
The RM should be stored in the original sealed container at the indicated temperature.
Instructions for use
It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.
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2. 每批次樣品需包含空白對照及平行樣(相對偏差≤10%);
3. 回收率應控制在85%-110%。
2. 解吸液體積1.0 mL,震蕩解吸30分鐘;
3. 色譜條件:毛細管柱(HP-5),柱溫80℃(3分鐘)-20℃/min升溫至200℃;
4. 定量方法:外標法定量。
2. 活性炭管采樣前后需密封避光保存(≤4℃冷藏);
3. 實驗中需佩戴防護手套,避免皮膚直接接觸解吸液(二硫化碳)。
以上信息僅供參考,請以相應標準的原文為準!