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滅菌磷(EC 17025)_5131-24-8
圖片僅供參考,具體產(chǎn)品以實物為準(zhǔn)!

滅菌磷(EC 17025)

BW902032 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨詢'}} ¥{{goodObj.sell_price || 0}} 咨詢 5131-24-8 25mg {{goodObj.date}} 秦境 {{item.norm}} 99.0% {{inventory}}
滅菌磷介紹:

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external7 accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.

Tel:029-85836892 Web:www.qjbzwz.com Email:[email protected]

Address:Jiawei Technology Industry Base, Aerospace East Road, Xi’an , Shaanxi Province


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標(biāo)準(zhǔn)名稱及標(biāo)準(zhǔn)號
GB/T 5750.9-2023《生活飲用水標(biāo)準(zhǔn)檢驗方法 第9部分:農(nóng)藥指標(biāo)》
適用范圍
適用于生活飲用水及其水源水中滅菌磷(CAS:5131-24-8)的檢測,涵蓋水樣的采集、保存、前處理及儀器分析流程。
核心檢測方法
采用氣相色譜-質(zhì)譜聯(lián)用法(GC-MS)。水樣經(jīng)固相萃取(SPE)富集凈化后,通過毛細(xì)管色譜柱分離,質(zhì)譜檢測器定性定量分析。
檢出限與定量限
方法檢出限(MDL)為0.02 μg/L,定量限(LOQ)為0.08 μg/L,滿足飲用水衛(wèi)生標(biāo)準(zhǔn)中關(guān)于滅菌磷的限量要求。
質(zhì)控樣品要求
每批次樣品需包含空白對照、加標(biāo)回收樣品和平行樣。加標(biāo)濃度應(yīng)為定量限的2-5倍,回收率需控制在70%-120%,相對標(biāo)準(zhǔn)偏差(RSD)≤15%。
關(guān)鍵實驗步驟
1. 樣品萃取:使用C18固相萃取柱,活化后上樣,流速控制在3-5 mL/min;
2. 洗脫與濃縮:用5 mL乙酸乙酯洗脫,氮吹濃縮至0.5 mL;
3. 儀器條件:色譜柱為HP-5MS(30 m×0.25 mm×0.25 μm),進(jìn)樣口溫度260℃,質(zhì)譜掃描模式為SIM。
特別說明
1. 滅菌磷易光解,樣品需避光保存并在48小時內(nèi)完成前處理;
2. 若水樣渾濁需先經(jīng)0.45 μm濾膜過濾;
3. 質(zhì)譜定性需滿足保留時間偏差±2%內(nèi),特征離子豐度比與標(biāo)準(zhǔn)品一致。

以上信息僅供參考,請以相應(yīng)標(biāo)準(zhǔn)的原文為準(zhǔn)!

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