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百里酚_89-83-8
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百里酚

BW905020 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨詢'}} ¥{{goodObj.sell_price || 0}} 咨詢 89-83-8 100mg {{goodObj.date}} 秦境 {{item.norm}} 99.6% {{inventory}}
百里酚介紹:

REFERENCE MATERIAL CERTIFICATE

Reference Material

This certificate is designed in accordance with ISO17034 and ISO Guide 31. This reference material (RM) was designed,produced andverified in accordance with ISO/IEC 17025, ISO 17034 and a registered qualitymanagement system ISO9001.

Product Name

Thymol

Product Code

BW905020

Lot Number

23071537

CAS No.

89-83-8

Mol. Formula

C10H14O

Mol. Weight

150.22

Certified on

21 Jul 2023

Expiry Date

20 Jul 2028

Storage Temp

20°C ± 4°C

Specification

100mg

CERTIFIED

Purity

CERTIFIED

Expanded Uncertainty (U)

Approved by

99.6%

1.0%

Method of Characterisation

GC/FID

Batch Information

Water Content: <0.1% (by Karl-Fischer-Titration)

Uncertainty

The certified value(s) and uncertainty(ies) aredetermined in accordance with ISO 17034 with an 95% confidence level (k=2).Uncertainty is based on the Total Combined Uncertainty, including uncertaintiesof characterisation, homogeneity and stability testing. Stability values are basedon real evidence opposed to simulation.

The producer certifies that this reference materialmeets the specification stated in this certificate until the expiry date,provided it is stored unopened at the recommended temperature herein. Productwarranties for this reference material are set out in the terms and conditionsof purchase.

Intended Use

This RM is intended for use in a laboratory as acalibration and quality control standard or in method development foranalytical techniques.

Safety

Proper precautions should be observed whilehandling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements arecalibrated with weights traceable to the national standards (DKD). Thecalibration of the balances is verified daily internally and annually by anexternal7 accredited calibration service. Chromatographic methods are traceableto the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RMhave been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealedcontainer at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum samplesize and if less material is used, to increase the certified uncertainty by afactor of two for half sample and four for a quarter of sample. If storageafter opening is necessary, the RM should be tightly closed and kept from lightand moisture. If the RM was in a sealed ampoule, it should be transferred to avial with minimum head space.


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標(biāo)準(zhǔn)名稱及標(biāo)準(zhǔn)號(hào)
標(biāo)準(zhǔn)名稱 食品安全國家標(biāo)準(zhǔn) 食品中百里酚殘留量的測(cè)定 氣相色譜-質(zhì)譜法
標(biāo)準(zhǔn)號(hào) GB 23200.113-2018
適用范圍
本標(biāo)準(zhǔn)適用于食品(包括植物源性食品、動(dòng)物源性食品等)中百里酚殘留量的檢測(cè),適用于進(jìn)出口產(chǎn)品及國內(nèi)食品監(jiān)管領(lǐng)域。
核心檢測(cè)方法
氣相色譜-質(zhì)譜聯(lián)用法(GC-MS)。前處理包括樣品粉碎、乙腈提取、弗羅里硅土柱凈化、氮吹濃縮等步驟,最終通過色譜柱分離與質(zhì)譜檢測(cè)定量分析。
檢出限與定量限
檢出限 0.005 mg/kg
定量限 0.01 mg/kg
質(zhì)控樣品要求
每批次樣品需包括空白樣品、加標(biāo)空白樣品(低、中、高濃度)及實(shí)際樣品平行分析。加標(biāo)回收率應(yīng)為70%-120%,相對(duì)標(biāo)準(zhǔn)偏差(RSD)≤15%。
關(guān)鍵實(shí)驗(yàn)步驟
1. 樣品提取:使用乙腈超聲輔助提取;
2. 凈化:弗羅里硅土柱去除干擾物質(zhì);
3. 氮吹濃縮:40℃下氮吹至近干;
4. 儀器條件:DB-5MS色譜柱,升溫程序80℃保持1min,以20℃/min升至260℃保持5min。
5. 質(zhì)譜檢測(cè):選擇離子監(jiān)測(cè)(SIM)模式,定量離子為m/z 135。
特別說明
1. 需注意樣品中酚類物質(zhì)的干擾,必要時(shí)增加雙波長(zhǎng)檢測(cè);
2. 實(shí)驗(yàn)室環(huán)境溫濕度需控制,避免有機(jī)溶劑揮發(fā)影響定量準(zhǔn)確性;
3. 標(biāo)準(zhǔn)溶液需現(xiàn)配現(xiàn)用,避光保存不超過24小時(shí)。

以上信息僅供參考,請(qǐng)以相應(yīng)標(biāo)準(zhǔn)的原文為準(zhǔn)!

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